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The Assignment of the Absolute Configuration by NMR Using Chiral Derivatizing Agents: A Practical Guide briefly explains the theoretical aspects necessary for understanding the methodology of new research in the field of Nuclear magnetic resonance spectroscopy (NMR), dedicating most of its space to covering the practical aspects of the assignment, with examples and spectra taken from the authors' own experiments. Upper-level undergraduates, graduate students, and chemical researchers will find this guide useful for their studies and practice.